A new method for collection and identification of gunshot residues from the hands of shooters.

نویسندگان

  • Edson L T Reis
  • Jorge E Souza Sarkis
  • Osvaldo N Neto
  • Claudio Rodrigues
  • Maurício H Kakazu
  • Sônia Viebig
چکیده

This work presents a novel collection method for gunshot residues (GSR) using a sampling procedure based on ethylenediaminetetraacetic acid (EDTA) solution as a complexing agent on moistened swabs. Detection was via a sector-field inductively coupled plasma mass spectrometry (HRICP-MS). The proposed collection and analytical method allowed detection of antimony (Sb), barium (Ba) and lead (Pb) after .38 shot tests. at detection limits of less than 1 microg L(-1) in four different areas of the hands of volunteers. This paper includes a discussion concerning hand areas near the thumb and forefinger as being more suitable for GSR collection as well as a comparison between differences observed using 2% diluted EDTA. 2% nitric acid solution, and simple deionized water as collecting solutions, proving the superior efficiency of EDTA in GSR recoveries.

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عنوان ژورنال:
  • Journal of forensic sciences

دوره 48 6  شماره 

صفحات  -

تاریخ انتشار 2003