A new method for collection and identification of gunshot residues from the hands of shooters.
نویسندگان
چکیده
This work presents a novel collection method for gunshot residues (GSR) using a sampling procedure based on ethylenediaminetetraacetic acid (EDTA) solution as a complexing agent on moistened swabs. Detection was via a sector-field inductively coupled plasma mass spectrometry (HRICP-MS). The proposed collection and analytical method allowed detection of antimony (Sb), barium (Ba) and lead (Pb) after .38 shot tests. at detection limits of less than 1 microg L(-1) in four different areas of the hands of volunteers. This paper includes a discussion concerning hand areas near the thumb and forefinger as being more suitable for GSR collection as well as a comparison between differences observed using 2% diluted EDTA. 2% nitric acid solution, and simple deionized water as collecting solutions, proving the superior efficiency of EDTA in GSR recoveries.
منابع مشابه
Evaluation of Cryofocusing Capillary Microextraction of Volatiles for Improved Detection of Organic Gunshot Residue on the Hands of Shooters
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عنوان ژورنال:
- Journal of forensic sciences
دوره 48 6 شماره
صفحات -
تاریخ انتشار 2003